Synthesis and Structure of A Liquid Crystal Compound: 1,4-bis(2,2,6,6-tetramethylpiperidin-4-yl)benzene

Volume 2, Issue 3, June 2017     |     PP. 105-113      |     PDF (450 K)    |     Pub. Date: June 20, 2017
DOI:    394 Downloads     7917 Views  

Author(s)

Yuanyuan Sun, Xi'an Manareco New Material Co., Ltd., Affiliated 71#, 2nd Jinye Rd, Gaoxin District, Xi'an, Shanxi, People’s Republic of China.

Abstract
The title compound, C24H40N2, was synthesized via etherification, Grignard reaction, dehydration and hydrogenation to produce 1,4-bis(2,2,6,6-tetramethylpiperidin-4-yl)benzene with a purity of more than 99. 95%．The overall yield was 70%．The structure of the target compound was confirmed by IR and single-crystal X-ray diffraction．

Keywords
1,4-bis(2,2,6,6-tetramethylpiperidin-4-yl)benzene; Crystalline structure; Liquid crystal

Cite this paper
Yuanyuan Sun, Synthesis and Structure of A Liquid Crystal Compound: 1,4-bis(2,2,6,6-tetramethylpiperidin-4-yl)benzene , SCIREA Journal of Chemistry. Volume 2, Issue 3, June 2017 | PP. 105-113.

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